日本語フィールド
著者:Yuka Mineyama, Ko Yoneda , Yasunori Yamada, and Masayuki Koikawa題名:Synthesis and Crystal Structure of Bis{2-[(2-hydroxymethylphenyl)iminomethyl]-4-nitro-phenolato}nickel(II) Monoacetonitrile発表情報:X-ray Structure Analysis Online 巻: 37 ページ: 85キーワード:概要:抄録:The title compound, [Ni(HL1-NO2)2]CH3CN, [H2L1-NO2 = 2-[2-(hydroxymethylphenyl)iminomethyl]-4-nitrophenol], was synthesized and characterized by single-crystal X-ray analysis. The compound crystallizes in the triclinic space group P\bar{1} with cell parameters a = 10.556(2)Å, b = 11.779(3)Å, c = 12.247(3)Å, = 86.412(10)°, = 71.135(8)°, = 73.009(8)°, V = 1377.2(5)Å3, Dcalcd = 1.549 g/cm3, Z = 2. The R1 [I > 2(I)] and wR2 (all data) values are 0.0362 and 0.1024, respectively, for all 5989 independent reflections. The tridentate ligands coordinate to the nickel atom as a mer-manner.英語フィールド
Author:Yuka Mineyama, Ko Yoneda , Yasunori Yamada, and Masayuki KoikawaTitle:Synthesis and Crystal Structure of Bis{2-[(2-hydroxymethylphenyl)iminomethyl]-4-nitro-phenolato}nickel(II) MonoacetonitrileAnnouncement information:X-ray Structure Analysis Online Vol: 37 Page: 85An abstract:The title compound, [Ni(HL1-NO2)2]CH3CN, [H2L1-NO2 = 2-[2-(hydroxymethylphenyl)iminomethyl]-4-nitrophenol], was synthesized and characterized by single-crystal X-ray analysis. The compound crystallizes in the triclinic space group P\bar{1} with cell parameters a = 10.556(2)Å, b = 11.779(3)Å, c = 12.247(3)Å, = 86.412(10)°, = 71.135(8)°, = 73.009(8)°, V = 1377.2(5)Å3, Dcalcd = 1.549 g/cm3, Z = 2. The R1 [I > 2(I)] and wR2 (all data) values are 0.0362 and 0.1024, respectively, for all 5989 independent reflections. The tridentate ligands coordinate to the nickel atom as a mer-manner.